Ai SolventVap 10L w/ -30°C Chiller & ULVAC PTFE Pump

    A$ 19,690.00 A$ 19,690.00 19690.0 AUD

    A$ 19,690.00

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    SKU# SE10-C30-DTC41


    Terms and Conditions

    ULVAC DTC-41 1.6 cfm Dual-Stage Chemical-Resist Diaphragm Pump

    A rotary evaporator is a device used in chemical laboratories for the efficient and gentle removal of solvents from samples by evaporation. The process of rotary evaporation is most often used to separate solvents with low boiling points, such a n-hexane or ethyl acetate, from compounds which are solid at room temperature and pressure. However, careful application also allows for the removal of a solvent from a sample containing a liquid compound, if there is minimal co-evaporation (azeotropic behavior) and a sufficient difference in boiling points at the chosen temperature and reduced pressure.

     

        

     

    Example:The following table is a list of a variety of substances ordered by increasing vapor pressure (in absolute units).

     

     

    The newly re-designed Ai SolventVap 10L (evaporating flask capacity) series rotary evaporators come with all PTFE valves for solvent-resistant operations. We also lowered the height of the height of assembled unit, for easy installation and ease of use and storage. Also come with them are vertical glassware and digital temperature/rotation control. Its optimized bath volume allows for rapid heat-up times. The condenser unit has specially designed glass tubes that utilize surface area extremely efficiently. That’s why our SolventVap evaporators consistently deliver reliable and reproducible process results that are usually reserved for more costly systems. Another important aspect of the SolventVap is the safety features, which includes dry-run protection, water bath over-temperature shut-off protection, and fuse protection.

    Rotary evaporator features a specially designed motor and worm gear, which provides constant rotation at speeds from 10 to 130 rpm. As the flask containing the solvent is rotated, it continually transfers a thin layer of liquid over the entire inner surface. This gives a very large surface area for evaporation, which is caused by the gentle heating from the water bath. The rotating system is fitted with a special seal that allows the apparatus to be placed under vacuum, effectively reducing the boiling point of the solvents and removing the vapor phase, making the process much more efficient. Each unit is also equipped with an easy-to-use vacuum release and a continuous feed system, which allows solvent to be constantly drawn into the rotating flask without needing to stop the operation.

    Digital water bath operates from ambient temperature to 99°C with PID temperature control stepping at 0.1°C increments. Heating coils are located directly inside the pan for the most efficient heating possible. A built-in overheat protector will shut down power, should the controller fail.

    Standard Glassware Set includes 10 liters round-bottomed evaporating flask, 5 liters round-bottomed receiving flask, and vertical condenser. Rotary evaporators with vertical glass condenser are great for distillation of solvents with higher boiling points.

    Features

    • Solvent-resistant PTFE and Viton gaskets, ensuring long time operation.
    • Specialized motor with extremely compact, intermeshed worm and worm gear provides precise driving for very quiet, vibration-free operation.
    • Downward-condensing vacuum connection design ensures safe vacuum operation.
    • Motorized water bath lifting for precise control.
    • Easy, straight-forward visual operation with digital speed and temperature display.
    • PID temperature controller ensures accurate temperature control is maintained.
    • One year warranty and lifetime US-based parts and service support.

    Your safety is important to us! Please use caution when operating. Users of glass reaction equipment must take all necessary precautions to avoid contact with rotating parts, particularly entanglement of loose clothing, hair, necklaces, or other jewelry. Under these circumstances, the winding action of the rotating parts can draw the user(s) into the apparatus, resulting in breakage of glassware, burns, and/or chemical exposure. Extra caution must also be taken when operating with air-reactive materials, especially under vacuum. A leak can draw air into the apparatus and cause a violent reaction to occur.

    Specifications

     Electrical requirements
     220-240V 50/60Hz single phase, 22A, 3800 watt (rotation motor: 250 watts)
     Evaporating flask
     Capacity: 10 liters
     Maximum load: Not to exceed 60% of the flask's capacity
     Sealing flange: 3.7" (95mm) diameter
     Rotation speed: 10 to 130 rpm
     Evaporating speed: 3.2 liters/hour (water), 6.5 liters/hour (alcohol)
     Receiving flask
     5 liters
     Condenser Glassware: Main + auxiliary triple-circulating cold traps, vertical
     Chilling fluid conneciton: 3/8" hose barb x 4 (2 on main + 2 on auxiliary)
     Working environment
     -15 to 35°C
     Water bath
     Temperature range: ambient to 99°C
     Temperature controller: digital
     Dimensions: 350 x 220 x 280 (WxDxH)
     Material: stainless steel
     Media: water
     Number of heaters: two
     Drain port: one
     Exterior liner: rubber
     Lifting: motorized
     Maximum lifting distance: 100 mm
     Vacuum
     Vacuum level: < 3 torrs / 0.4 kPa
     Vacuum sealing: PTFE + Vinton gaskets
     Vacuum connection: 3/8" hose barb x 1 on main condenser
     Swivel casters
     Four, built-in with locks
     Safety Dry-run, over-temp shut-off, built-in circuit breakers
     Shipping weight 91 kg (evaporator), 45 kg (glassware)
     Unit dimensions
     910 x 560 x 1700 mm (WxDxH)
     Shipping dimensions 990 x 560 x 1120 mm (evaporator), 760 x 640 x 710 mm (glassware) (WxDxH)

     

     

     




     

    Standard package

     Part description

     Quantity

    Part image

     Ai C30-17 -30°C/-22°F 17L capacity recirculating chiller and accessories1 set
     ULVAC DTC-41 1.6 cfm 7.5 torr 2-head diaphragm pump and vacuum hose1 set 
     Ai SolventVap 10L rotary evaporator and water bath
    1 set
     Vertical main and auxiliary condensers, glass
    2 pcs
     10L round shaped rotating evaporating flask, glass
    1 pc
     5L receiving flask with detachable drain port
    1 pc
     Three-way tee vapor buffering flask, glass
    1 pc
     Vapor duct and evaporation flask seal (pre-installed)
    1 set 
     Receiving flask glass vacuum port with PTFE open/close valve 2 sets
     Glass material feeding port with PTFE open/close valve1 set 
     PTFE extension feeding hose1 pc 
     Stainless steel pole and mechanical vacuum gauge
    2 pcs
     Silicone vacuum tubing
    10 ft
     Rubber-wrapped condenser & receiving flask support and bracket3 pcs
     Flask quick clamp and centering rings
    7 sets
     GL18 connector
    5 sets
     Evaporating flask cap spanner, allen key & hex screws
    1 set  
     Ai plexiglass cover for SolventVap 10L1 pc
     User's manual1 pc

     

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